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Updated: Jan 2, 2026

Quasistatic Mechanical Testing for Computer-Aided Design and Manufacturing Occlusal Veneers Cemented to Milled Dentin Analog Material
Published on: December 20, 2024
Effect of etching the coronal dentin with the rubbing technique on the microtensile bond strength of a universal
Naji Kharouf1,2, Gautier Rapp2, Davide Mancino1,2
1Inserm UMR_S 1121, Biomaterials and Bioengineering, University of Strasbourg, France.
Background:
The adhesion of composite resins to the dentin substrate is influenced by the treatment of the smear layer. While etch-and-rinse systems require dentin to be conditioned with phosphoric acid, self-etching systems preserve the smear layer by incorporating it into the adhesive layer.
Objectives:
The objective of this study was to evaluate the influence of etching with the rubbing technique on the microtensile bond strength (μTBS) of a universal adhesive to dentin.
Material And Methods:
Eighteen extracted teeth were selected. Two etch-and-rinse techniques (with and without rubbing) and a self-etching technique were used to bond the dentin surfaces with a universal adhesive system. After 24 h, the bonded samples were prepared for the μTBS testing. The specimens were loaded with a tensile force at a crosshead speed of 0.5 mm/min until failure. The scanning electron microscope (SEM) analyses were used to reveal the failure modes. The data were statistically analyzed with the one-way analysis of variance (ANOVA) and χ2 tests.
Results:
The etch-and-rinse system with rubbing produced significantly lower bond strength (42.11 ±9.26 MPa,) than the etch-and-rinse system without rubbing (47.30 ±8.12 MPa) and significantly higher bond strength than the self-etching system (38.07 ±9.49 MPa).
Conclusions:
Under the conditions of this study, dentin etched with phosphoric acid for 3 s in the etchandrinse mode with the rubbing technique for a universal adhesive system decreases the μTBS of the composite to dentin.

