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Updated: Jan 2, 2026

Reverse Microemulsion-mediated Synthesis of Monometallic and Bimetallic Early Transition Metal Carbide and Nitride Nanoparticles
Published on: November 27, 2015
Reduced to Hierarchy: Carbon Filament-Supported Mixed Metal Oxide Nanoparticles
G V Manohara1,2, Andrew Whiting1, H Chris Greenwell1
1Department of Chemistry and Department of Earth Sciences, Durham University, Durham DH1 3LE, U.K.
Abstract:
We describe a one-pot synthesis method for carbon filament-supported mixed metal oxide nanoparticles. The thermal intracrystalline reaction of adamantanecarboxylate ions confined inside interlayer galleries of layered double hydroxide materials under a reducing atmosphere (H2) leads to carbon filaments forming in situ within the material. Raman spectroscopy and combined microscopy techniques show the formation of hybrid organic-inorganic carbon filaments with the mixed metal oxide particles interleaved.

