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Heat Treatments and Critical Quenching Rates in Additively Manufactured Al-Si-Mg Alloys
Leonhard Hitzler1, Stephan Hafenstein1, Francisca Mendez Martin2
1Institute of Materials Science and Mechanics of Materials, Technical University Munich, 85748 Garching, Germany.
Materials (Basel, Switzerland)
|February 9, 2020
Summary
Laser powder-bed fusion (LPBF) of Al-Si-Mg alloys creates fine microstructures. Direct aging post-LPBF is less effective than in cast materials due to higher quenching rate requirements for precipitation hardening.
Area of Science:
- Materials Science
- Metallurgy
- Additive Manufacturing
Background:
- Laser powder-bed fusion (LPBF) is a key metal additive manufacturing technique.
- LPBF processing of Al-Si-Mg alloys yields fine microstructures and supersaturated solid solutions.
- Inherent heat treatment during LPBF promotes beneficial alloying element clustering.
Purpose of the Study:
- To investigate the effectiveness of direct aging as a post-heat treatment for LPBF Al-Si-Mg alloys.
- To compare the precipitation hardening behavior of LPBF Al-Si-Mg with cast counterparts.
- To understand the influence of quenching rates on the mechanical properties of LPBF Al-Si-Mg.
Main Methods:
- Laser powder-bed fusion (LPBF) of Al-Si-Mg alloys.
- Direct aging heat treatment applied to as-built samples.
- Microstructural analysis and hardness testing.
- Comparison with cast Al-Si-Mg reference samples.
Main Results:
- Direct aging of LPBF Al-Si-Mg samples did not surpass the hardness of as-built samples.
- LPBF Al-Si-Mg exhibited a significantly higher sensitivity to quenching rates compared to cast samples.
- Achieving similar hardness required 2-3x higher quenching rates for LPBF samples after solution annealing.
Conclusions:
- The fine microstructure and short diffusion paths in LPBF Al-Si-Mg alloys complicate achieving the necessary metastable supersaturation for effective precipitation hardening.
- Higher quenching rates are critical for successful post-heat treatment of LPBF Al-Si-Mg alloys.
- Challenges in achieving optimal precipitation hardening may be more pronounced in larger LPBF components.

