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Non-equilibrium Microwave Plasma for Efficient High Temperature Chemistry
Published on: August 1, 2017
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Progress Towards a Gas-Flow Standard using Microwave and Acoustic Resonances.
Jodie G Pope1, Keith A Gillis1, Michael R Moldover1
1Fluid Metrology Group, NIST, Gaithersburg, MD 20899, USA.
Summary
A new gas flow standard uses microwave and acoustic resonances to precisely measure volume and density. This novel pressure, volume, speed of sound, and time (PVwt) standard calibrates critical flow venturis with high accuracy.
Area of Science:
- Metrology
- Fluid Dynamics
- Acoustics
Background:
- Development of a novel gas flow standard is crucial for accurate flow measurements.
- Existing standards require precise knowledge of volume and gas density.
- Microwave and acoustic resonance techniques offer potential for high-accuracy measurements.
Purpose of the Study:
- To develop and validate a novel gas flow standard using microwave and acoustic resonances.
- To establish a primary standard for pressure, volume, speed of sound, and time (PVwt).
- To calibrate critical flow venturis (CFVs) using the developed gas flow standard.
Main Methods:
- Utilized microwave resonances to determine the pressure- and temperature-dependent volume (V_BBB) of a 1.85 m³ steel vessel.
- Employed acoustic resonances and a novel positive feedback system to measure the average gas density and "acoustic mass" (M_acst).
- Calibrated three NIST working standard critical flow venturis using the V_BBB, pressure, and acoustic resonance measurements.
Main Results:
- The V_BBB was determined with an expanded uncertainty of 0.022%.
- Acoustic mass measurements agreed with gravimetric measurements within 0.04%, even with temperature gradients.
- Independent calibrations of critical flow venturis agreed within 0.053%, demonstrating the standard's accuracy and reproducibility.
Conclusions:
- The novel gas flow standard, based on microwave and acoustic resonances, provides accurate measurements of volume and gas density.
- The developed PVwt primary standard successfully calibrated working standards, showing high agreement and reproducibility.
- The feasibility of dynamic tracking for flow measurements was demonstrated, indicating potential for real-time flow monitoring.
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