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Updated: Dec 27, 2025

Solvothermal Synthesis of MIL-96 and UiO-66-NH2 on Atomic Layer Deposited Metal Oxide Coatings on Fiber Mats
Published on: June 13, 2018
Solution Combustion Synthesis: Towards a Sustainable Approach for Metal Oxides
Emanuel Carlos1, Rodrigo Martins1, Elvira Fortunato1
1Materials Science Department, CENIMAT/i3N, Faculdade de Ciências e Tecnologia (FCT), Universidade NOVA de Lisboa (UNL) and CEMOP/UNINOVA, 2829-516, Caparica, Portugal.
Abstract:
Solution combustion synthesis (SCS) has been widely used to produce simple and complex oxides with a desired morphology (size and shape). SCS is valuable due to low cost, simplicity and energy efficient synthesis. To guarantee the best molecular-level mixing of reactants in an aqueous or solvent-based solution some parameters need to be controlled, such as fuel type, metal cations precursors, stoichiometry ratio (φ), pH effect, atmosphere and initiation type. These determine the final properties of the oxide materials, providing the potential to reach different morphologies, which are essential for their final applications. This Review article focuses on the crucial parameters in SCS and how these affect the overall materials properties from nanostructures to thin films. To finalize, special attention is given to the application of SCS to form metal oxide thin films at low temperature and their application in thin film transistors (TFTs).
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