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Updated: Dec 24, 2025

Quantitative Hardness Measurement by Instrumented AFM-indentation
Published on: November 22, 2016
Nano-Indentation Response of Ultrahigh Molecular Weight Polyethylene (UHMWPE): A Detailed Analysis
Tanveer Iqbal1, S S Camargo2, Saima Yasin1
1Department of Chemical, Polymer & Composite Materials Engineering, University of Engineering & Technology, KSK Campus, Lahore 54890, Pakistan.
Abstract:
Nano-indentation, a depth sensing technique, is a useful and exciting tool to investigate the surface mechanical properties of a wide range of materials, particularly polymers. Knowledge of the influence of experimental conditions employed during nano-indentation on the resultant nano-mechanical response is very important for the successful design of engineering components with appropriate surface properties. In this work, nano-indentation experiments were carried out by selecting various values of frequency, amplitude, contact depth, strain rate, holding time, and peak load. The results showed a significant effect of amplitude, frequency, and strain rate on the hardness and modulus of the considered polymer, ultrahigh molecular weight polyethylene (UHMWPE). Load-displacement curves showed a shift towards the lower indentation depths along with an increase in peak load by increasing the indentation amplitude or strain rate. The results also revealed the strong dependence of hardness and modulus on the holding time. The experimental data of creep depth as a function of holding time was successfully fitted with a logarithmic creep model (R2 ≥ 0.98). In order to remove the creeping effect and the nose problem, recommended holding times were proposed for the investigated polymer as a function of different applied loads.
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