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Related Experiment Video

Updated: Dec 16, 2025

$High Pressure Single Crystal Diffraction at PX^2$

High Pressure Single Crystal Diffraction at PX^2

Published on: January 16, 2017

A simple system for neutron diffraction at 4 K and elevated pressures.

Christopher J Ridley¹, Nicholas P Funnell¹, Colin Offer¹

¹ISIS Neutron and Muon Source, Rutherford Appleton Laboratory, Chilton, Didcot OX11 0QX, United Kingdom.

The Review of Scientific Instruments

|July 3, 2020

Summary

This summary is machine-generated.

A novel cryogen-free refrigerator system for the Paris-Edinburgh press achieves 3 GPa at 4-300 K. This versatile system is compatible with neutron diffraction instruments, enabling new high-pressure research.

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High-Pressure NMR Experiments for Detecting Protein Low-Lying Conformational States

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High-Pressure NMR Experiments for Detecting Protein Low-Lying Conformational States

High-Pressure NMR Experiments for Detecting Protein Low-Lying Conformational States

Published on: June 29, 2021

Area of Science:

Materials Science
Condensed Matter Physics
High-Pressure Science

Background:

High-pressure research requires specialized equipment for generating extreme conditions.
Cryogen-free systems offer advantages in terms of operational simplicity and cost-effectiveness.
The Paris-Edinburgh press is a well-established tool for high-pressure studies.

Purpose of the Study:

To develop and present a unique cryogen-free closed-cycle refrigerator system.
To demonstrate the system's compatibility with neutron powder-diffraction instruments.
To showcase the system's capability for generating high pressures and wide temperature ranges.

Main Methods:

Utilized a beryllium-copper VX1 variant of the Paris-Edinburgh press.
Integrated a cryogen-free closed-cycle refrigerator.
Designed for compatibility with the PEARL neutron powder-diffraction instrument and other ISIS facility instruments.

Main Results:

Achieved approximately 3 GPa on a 66 mm³ sample volume.
Operated across a temperature range of 4 K to 300 K.
Successfully collected representative neutron powder-diffraction data on MnF₂ at 13 K and 2.4 GPa.

Conclusions:

The developed system offers a versatile and accessible platform for high-pressure research.
Its compatibility with multiple neutron-diffraction instruments enhances its utility.
This cryogen-free system opens new avenues for studying materials under extreme conditions.