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Structure of C32H34N2O5S2: corrigendum.

¹Noyes Laboratory of Chemical Physics, California Institute of Technology, Pasadena 91125.

Acta Crystallographica. Section C, Crystal Structure Communications

|May 15, 1988

Summary

This study revises the crystallographic description of a heterocyclic compound, reclassifying its structure from triclinic to monoclinic (C2/c) space group. This correction provides accurate structural data for the molecule.

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Use of software to search for higher symmetry: space group C2.

Acta crystallographica. Section B, Structural science·2001

Area of Science:

Crystallography
Structural Chemistry
Organic Chemistry

Background:

The initial crystallographic analysis of a 13-membered heterocyclic compound reported a triclinic (P1) structure.
This prior description contained specific lattice parameters and space group information.

Purpose of the Study:

To re-evaluate and correct the crystallographic description of the heterocyclic compound.
To provide an accurate structural classification and refined crystallographic data.

Main Methods:

Re-analysis of the compound's crystal structure.
Determination of the correct crystallographic space group and lattice parameters.
Calculation of atomic coordinates for the revised structure.

Main Results:

The compound's structure was accurately described as monoclinic, space group C2/c.
New lattice parameters (a', b', c') and angle (beta') were determined.
The molecule was found to lie on an exact twofold axis, refining previous assumptions.

Conclusions:

The revised monoclinic (C2/c) description supersedes the previous triclinic (P1) assignment.
Accurate crystallographic data, including coordinates, are provided for the heterocyclic compound.
The precise positioning of the molecule on a twofold axis clarifies its symmetry properties.

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