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Insight into β-cyclodextrin polymer microsphere as a potential filtration reducer in water-based drilling fluids for
Hanyi Zhong1, Xin Gao1, Zhengsong Qiu1
1Key Laboratory of Unconventional Oil & Gas Development (China University of Petroleum (East China), Ministry of Education, Qingdao, 266580, China; School of Petroleum Engineering, China University of Petroleum (East China), Qingdao, Shandong, 266580, China.
New beta-cyclodextrin polymer microspheres (β-CDPMs) offer effective filtration control for water-based drilling fluids at high temperatures. These microspheres function optimally above 160°C, forming dense filter cakes via nanoparticle generation.
Area of Science:
- Materials Science
- Chemical Engineering
- Petroleum Engineering
Background:
- Effective filtration control of water-based drilling fluids is crucial in high-temperature drilling engineering.
- Existing filtration reducers often face limitations in extreme thermal environments.
Purpose of the Study:
- To synthesize and evaluate beta-cyclodextrin polymer microspheres (β-CDPMs) as novel filtration reducers for high-temperature applications.
- To elucidate the mechanism behind the filtration control performance of β-CDPMs at elevated temperatures.
Main Methods:
- Synthesis of β-CDPMs using inverse emulsion polymerization of β-cyclodextrin and epichlorohydrin.
- Standard American Petroleum Institute filtration tests were conducted at various temperatures.
- Analysis of filter cake structure and composition after thermal aging.
Main Results:
- β-CDPMs demonstrated enhanced filtration control specifically at temperatures above 160 °C.
- The material exhibited thermal stability up to 240 °C with minimal impact on rheology.
- Hydrothermal reactions above 160 °C generated nano carbon spheres and nanostructured composites, forming dense filter cakes.
Conclusions:
- β-CDPMs provide a viable solution for high-temperature filtration control in water-based drilling fluids.
- The formation of stable nanoparticles via hydrothermal reactions is key to the filtration control mechanism.
- This study presents a novel approach for managing fluid filtration in challenging downhole conditions.
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