Related Experiment Video
Updated: Dec 2, 2025

10:10
Neutron Crystallography Data Collection and Processing for Modelling Hydrogen Atoms in Protein Structures
Published on: December 1, 2020
5.4K
A simple method to prepare deuterated targets for experiments relevant to nuclear astrophysics
1Saha Institute of Nuclear Physics, HBNI, 1/AF Bidhannagar, Salt Lake, Kolkata 700064, India.
The Review of Scientific Instruments
|November 3, 2020
Summary
A new method simplifies deuterated polyethylene target preparation, avoiding cryogenic freezing. This technique utilizes thermal expansion differences for easy target removal and characterization.
Area of Science:
- Materials Science
- Nuclear Physics
Background:
- Deuterated polyethylene targets are crucial for nuclear physics research.
- Existing preparation methods can be complex and require cryogenic conditions.
Purpose of the Study:
- To develop a simple and efficient method for preparing deuterated polyethylene targets.
- To enable convenient target removal without cryogenic freezing.
Main Methods:
- Utilizing the difference in thermal expansion between deuterated polyethylene and a glass casting surface.
- Determining target thickness via alpha (α) energy loss.
- Verifying material retention using Fourier-transform infrared spectroscopy and attenuated total reflection.
Main Results:
- Achieved target thicknesses ranging from 100 µg/cm² to 350 µg/cm².
- Thickness variation within the foils was controlled between 4% and 10%.
- Confirmed material retention properties of the deuterated foils.
Conclusions:
- The described method offers a straightforward and efficient approach to deuterated polyethylene target preparation.
- The technique facilitates easy target removal and provides well-characterized targets for research.
Related Concept Videos
¹H NMR of Labile Protons: Deuterium (²H) Substitution
1.2K
This lesson illustrates the role of deuterium substitution in simplifying the NMR spectrum of compounds comprising labile protons. One method employed is the use of deuterium. Amongst the three isotopes of hydrogen, deuterium (2H) has a nucleus composed of one proton and one neutron. When the D2O solvent is added to a pure dry ethanol solution, its labile proton is substituted with deuterium.
1.2K
Chemical Shift: Internal References and Solvent Effects
1.1K
In an NMR sample, precise measurement of the absolute absorption frequencies of nuclei is difficult. A standard internal reference compound is added, and the frequency difference between the reference signal and sample signals is measured.
The internal reference compound generally used in NMR spectroscopy is tetramethylsilane (TMS). TMS is preferred because it is chemically inert, soluble in NMR solvents, and easily removable. Also, the highly shielded methyl protons in TMS yield an intense...
The internal reference compound generally used in NMR spectroscopy is tetramethylsilane (TMS). TMS is preferred because it is chemically inert, soluble in NMR solvents, and easily removable. Also, the highly shielded methyl protons in TMS yield an intense...
1.1K
Double Resonance Techniques: Overview
524
Double resonance techniques in Nuclear Magnetic Resonance (NMR) spectroscopy involve the simultaneous application of two different frequencies or radiofrequency pulses to manipulate and observe two distinct nuclear spins. One important application of double resonance is spin decoupling, which selectively suppresses coupling with one type of nucleus while observing the NMR signal from another nucleus, simplifying the spectrum and enhancing resolution.
Spin decoupling is usually achieved by...
Spin decoupling is usually achieved by...
524
¹³C NMR: Distortionless Enhancement by Polarization Transfer (DEPT)
1.4K
When proton-coupled carbon-13 spectra are simplified by a broadband proton decoupling technique, structural information about the coupled protons is lost. Distortionless enhancement by polarization transfer (DEPT) is a technique that provides information on the number of hydrogens attached to each carbon in a molecule. While the DEPT experiment utilizes complex pulse sequences, the pulse delay and flip angle are specifically manipulated. The resulting signals have different phases depending on...
1.4K

