New bulk-fill composite system with high irradiance light polymerization: Integrity and degree of conversion

The study used optical coherence tomography (OCT) and micro Raman microscopy (mRM) to investigate internal defect (ID) and degree of conversion (DC) of two bulk-fill composite systems with high-irradiance or conventional light polymerization settings.

The ID and DC of the new bulk-fill composites; Tetric PowerFill (PwrPst) and Tetric PowerFlow (PwrFlw) were compared with the predecessor bulk-fill composites; Tetric EvoCeram Bulkfill (EvoPst) and Tetric EvoFlow Bulkfill (EvoFlw), using LED light curing unit in two settings; normal (LED-Nrm: 1000 mW/cm², 10-s) or PowerCure (LED-Pwr: 3000 mW/cm², 3-s). ID formation was observed in bonded cylindrical composite cavities (4-mm depth, 3-mm diameter) using Yoshida Dental OCT. From the vertically projected 2D image, ID area percentage (ID-A%) was calculated. DC at the top and bottom and bottom/top DC ratio (DC-R%) of 4-mm thick discs was calculated using mRM. All data were statistically analyzed at significance level of α = 0.05.

Flowable composites in LED-Pwr showed smaller ID frequencies than other groups (PwrFlw: 0/8, EvoFlw: 2/8) (p < 0.05). Composite type significantly affected ID-A%, DC and DC-R% (p < 0.001), while light settings significantly affected ID-A% but not DC and DC-R% (p > 0.05). In both light settings, EvoPst showed the lowest DC-R% (<80%).

Internal defect and degree of conversion of bulk-fill composites were affected by their composition and light settings. There was a tendency for less defects and better polymerization for the flowable bulk-fills. The new flowable bulk-fill composite with 3-seconds high irradiance light curing showed no defect formation.