Optimization of Preparation Conditions for Side-Emitting Polymer Optical Fibers Using Response Surface Methodology

Polymer optical fibers (POFs) were used for preparing side-emitting polymer optical fibers (SPOFs), which were processed with acetone and n-hexane combined in selected proportions by a solvent treatment method. The effects of the volume ratio of acetone to n-hexane and treatment time on response variable factors were investigated. The center composite design (CCD) based response surface methodology (RSM), a quadratic model, and a two-factor interaction model were developed to relate the preparation variables of illumination intensity, breaking strength, and rigidity. According to analysis of variance (ANOVA), the factors affecting the optimization of each response factor were determined. The predicted values after process optimization were found to be highly similar to the experimental values. The optimal conditions for the preparation of SPOF were as follows: the volume ratio of acetone to hexane was 1.703, and the treatment time was 2.716 s. The three response variables of SPOF prepared under the optimal conditions were: illumination intensity 19.339 mV, breaking strength 5.707 N, and rigidity 572.013 N·mm².