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Ultrasonic Time-of-Flight Computed Tomography for Investigation of Batch Crystallisation Processes.

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Summary

This study demonstrates ultrasound tomography for real-time monitoring of industrial crystallization processes. The system effectively tracks process dynamics and detects malfunctions, enhancing operational efficiency.

Keywords:
Fréchet kernelsbatch crystallisationcalcium carbonate crystallisationmonitoring crystallisationquality assurance tooltime-of-flight (TOF)transmission tomographytravel-timeultrasound computed tomography (USCT)

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Area of Science:

  • Chemical Engineering
  • Process Monitoring
  • Materials Science

Background:

  • Crystallization is vital in industrial processes, necessitating efficient monitoring for enhanced performance.
  • Ultrasound techniques are explored for particle sizing in liquid suspensions during crystallization.
  • Ultrasound tomography offers spatial insights, surpassing single-measurement systems for process analysis.

Purpose of the Study:

  • To investigate the application of ultrasound tomography for real-time monitoring of batch crystallization.
  • To assess the system's capability in capturing process dynamics and identifying malfunctions.
  • To evaluate the influence of injection rate and stirring speed on crystallization using this technology.

Main Methods:

  • Batch crystallization experiments were conducted in a lab-scale reactor using calcium carbonate.
  • A contactless ultrasound tomography system with 32 piezoelectric transducers (40 kHz central frequency) was employed in transmission mode.
  • Real-time tomographic imaging was performed, analyzing the effects of varying injection rates and stirring speeds.

Main Results:

  • The ultrasound tomography system successfully provided real-time spatial information during the crystallization process.
  • The system demonstrated its capability to monitor process dynamics, including the impact of control parameters like injection rate and stirring speed.
  • Potential for detecting process malfunctions was indicated through the obtained imaging data.

Conclusions:

  • Ultrasound tomography is a viable technique for effective real-time monitoring of industrial crystallization.
  • The system provides valuable insights into process dynamics and can aid in identifying operational issues.
  • This technology offers a non-invasive method to enhance control and efficiency in crystallization processes.