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Tailoring Microstructure and Mechanical Properties of Additively-Manufactured Ti6Al4V Using Post Processing
Yaron Itay Ganor1,2,3, Eitan Tiferet1,2, Sven C Vogel4
1Nuclear Research Center-Negev, P.O. Box 9001, Beer-Sheva 84190, Israel.
Materials (Basel, Switzerland)
|February 12, 2021
Summary
Lowering the hot isostatic pressing (HIP) temperature for additively manufactured titanium (Ti-6Al-4V) improves elongation and fatigue life while retaining strength. This suggests a revised standard HIP temperature for electron beam melted Ti64 components.
Area of Science:
- Materials Science
- Metallurgical Engineering
- Additive Manufacturing
Background:
- Additively manufactured Ti-6Al-4V (Ti64) offers high strength but often has limited elongation compared to conventionally produced materials.
- Post-processing is crucial for tailoring mechanical properties of 3D-printed Ti64 components for specific applications.
Purpose of the Study:
- To investigate the effects of post-processing, specifically heat treatments and hot isostatic pressing (HIP) cycles, on the microstructure and mechanical properties of electron beam melted Ti64.
- To determine optimal processing parameters for enhancing elongation and fatigue resistance without significantly compromising strength.
Main Methods:
- Electron beam melting (EBM) was used to produce Ti64 samples.
- Samples underwent various heat treatments up to 1000 °C and two distinct HIP cycles (780 °C and 920 °C).
- Neutron diffraction was employed to analyze phase content during heating, while mechanical properties (Vickers hardness, 0.2% proof stress, ultimate stress, elongation) and fatigue resistance were evaluated.
Main Results:
- Lowering the HIP temperature to 780 °C maintained the fine microstructure and high proof stress of as-built Ti64, significantly increasing elongation (~14%) and improving fatigue life.
- A higher HIP temperature (920 °C) resulted in a coarser microstructure and slightly reduced mechanical strength but still offered superior elongation (~6%) and fatigue resistance compared to the 780 °C HIP.
- Heat treatment at 1000 °C drastically altered the microstructure, leading to increased elongation but a notable decrease in proof stress.
Conclusions:
- The study indicates that a lower HIP holding temperature (780 °C) is beneficial for additively manufactured Ti64 produced by EBM, enhancing ductility and fatigue performance.
- Results suggest that the standard ASTM HIP temperature for Ti64 produced via EBM may need to be revised downwards to optimize material properties.
- Optimizing post-processing parameters like HIP temperature is key to unlocking the full potential of additively manufactured titanium alloys.

