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Updated: Nov 12, 2025

Utilization of Stop-flow Micro-tubing Reactors for the Development of Organic Transformations

Utilization of Stop-flow Micro-tubing Reactors for the Development of Organic Transformations

Published on: January 4, 2018

Electrosynthesis in Laminar Flow Using a Flow Microreactor.

Naoki Shida¹, Yuto Nakamura¹, Mahito Atobe¹

¹Department of Chemistry and Life Science, Yokohama National University, 79-5 Tokiwadai, Hodogaya-ku, Yokohama, Kanagawa, Japan.

Chemical Record (New York, N.Y.)

|March 18, 2021

Summary

This summary is machine-generated.

Integrating electrosynthesis with microflow reactors enables enhanced selectivity and control in organic synthesis. This approach offers unique advantages over traditional batch methods for various electrochemical reactions.

Keywords:

Electron transfer Electrosynthesis Flow Microreactor Parallel Laminar Flow Redox Chemistry

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Last Updated: Nov 12, 2025

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Published on: August 28, 2017

Area of Science:

Organic Chemistry
Electrochemistry
Chemical Engineering

Background:

Electrosynthesis and microflow synthesis are vital techniques in modern organic chemistry.
Combining these methods offers synergistic benefits for chemical reactions.

Purpose of the Study:

To summarize research on integrated electrosynthesis in flow microreactors.
To highlight the advantages of this combined technique over conventional batch methods.

Main Methods:

Development of an electrochemical microflow system with a micrometer-scale electrode gap.
Utilizing laminar flow within the microreactor for precise control.
Demonstration of various electrochemical systems and reactions.

Main Results:

Achieved unprecedented chemo- and electrochemical selectivity due to laminar flow.
Showcased unique applications including self-supported electrolysis and in situ generation of active species.
Demonstrated spatiotemporal control of electropolymerization and combinatorial screening.

Conclusions:

Electrosynthesis in flow microreactors provides superior selectivity and control.
This integrated technique enables novel electrochemical systems and efficient reaction condition screening.