Jove
Visualize
Contact Us
JoVE
x logofacebook logolinkedin logoyoutube logo
ABOUT JoVE
OverviewLeadershipBlogJoVE Help Center
AUTHORS
Publishing ProcessEditorial BoardScope & PoliciesPeer ReviewFAQSubmit
LIBRARIANS
TestimonialsSubscriptionsAccessResourcesLibrary Advisory BoardFAQ
RESEARCH
JoVE JournalMethods CollectionsJoVE Encyclopedia of ExperimentsArchive
EDUCATION
JoVE CoreJoVE BusinessJoVE Science EducationJoVE Lab ManualFaculty Resource CenterFaculty Site
Terms & Conditions of Use
Privacy Policy
Policies

Related Concept Videos

X-ray Crystallography02:18

X-ray Crystallography

24.8K
The size of the unit cell and the arrangement of atoms in a crystal may be determined from measurements of the diffraction of X-rays by the crystal, termed X-ray crystallography.
Diffraction
Diffraction is the change in the direction of travel experienced by an electromagnetic wave when it encounters a physical barrier whose dimensions are comparable to those of the wavelength of the light. X-rays are electromagnetic radiation with wavelengths about as long as the distance between neighboring...
24.8K
X-ray Diffraction of Biological Samples01:10

X-ray Diffraction of Biological Samples

4.2K
X-ray diffraction or XRD is an analytical tool that utilizes X-rays to study ordered structures such as crystalline organic and inorganic samples, polycrystalline materials, proteins, carbohydrates, and drugs.
According to Bragg's law, when X-rays strike the sample positioned on a stage, the rays are  scattered by the electron clouds around the sample atoms. The  X-ray diffraction or scattering is caused by constructive interference of the X-ray waves that reflect off the internal...
4.2K

You might also read

Related Articles

Articles linked to this work by shared authors, journal, and citation graph.

Sort by
Same author

Computer-based patient simulations: hospital pharmacists' performance and opinions.

American journal of hospital pharmacy·1992
Same author

Quantum States and atomic structure of silicon surfaces.

Science (New York, N.Y.)·1986
Same author

Continuing education support as a fringe benefit.

American journal of hospital pharmacy·1982
Same author

Community action in venereal disease education.

The Journal of school health·1973

Related Experiment Video

Updated: Nov 8, 2025

Measurements of Long-range Electronic Correlations During Femtosecond Diffraction Experiments Performed on Nanocrystals of Buckminsterfullerene
08:44

Measurements of Long-range Electronic Correlations During Femtosecond Diffraction Experiments Performed on Nanocrystals of Buckminsterfullerene

Published on: August 22, 2017

7.9K

A re-evaluation of diffraction from Si(111) 7 × 7: decoding the encoded phase information in the 7 × 7 diffraction

J E Demuth1

  • 1Naples, Florida 34114. jedemuth7x7@gmail.com.

Physical Chemistry Chemical Physics : PCCP
|April 20, 2021
PubMed
Summary

This study re-evaluates the Si(111) 7 × 7 surface structure using advanced crystallography, revealing new models beyond the dimer-adatom-stacking fault (DAS) structure. New polymorphs with potential magnetic properties are identified, challenging existing surface science paradigms.

More Related Videos

Synchrotron X-ray Microdiffraction and Fluorescence Imaging of Mineral and Rock Samples
10:12

Synchrotron X-ray Microdiffraction and Fluorescence Imaging of Mineral and Rock Samples

Published on: June 19, 2018

9.3K
High Pressure Single Crystal Diffraction at PX^2
11:32

High Pressure Single Crystal Diffraction at PX^2

Published on: January 16, 2017

21.8K

Related Experiment Videos

Last Updated: Nov 8, 2025

Measurements of Long-range Electronic Correlations During Femtosecond Diffraction Experiments Performed on Nanocrystals of Buckminsterfullerene
08:44

Measurements of Long-range Electronic Correlations During Femtosecond Diffraction Experiments Performed on Nanocrystals of Buckminsterfullerene

Published on: August 22, 2017

7.9K
Synchrotron X-ray Microdiffraction and Fluorescence Imaging of Mineral and Rock Samples
10:12

Synchrotron X-ray Microdiffraction and Fluorescence Imaging of Mineral and Rock Samples

Published on: June 19, 2018

9.3K
High Pressure Single Crystal Diffraction at PX^2
11:32

High Pressure Single Crystal Diffraction at PX^2

Published on: January 16, 2017

21.8K

Area of Science:

  • Surface Science
  • Crystallography
  • Materials Science

Background:

  • The Si(111) 7 × 7 surface reconstruction is a fundamental system in surface science.
  • Previous structural models, including the dimer-adatom-stacking fault (DAS) model, have limitations due to simplified analyses and experimental uncertainties.

Purpose of the Study:

  • To analyze diffraction features of the Si(111) 7 × 7 surface.
  • To relate these features to various structural models, proposing new ones that better explain experimental data.
  • To investigate potential magnetic surface states in new structural polymorphs.

Main Methods:

  • Multivariate analysis of diffraction data.
  • Projection rod method for surface crystallography.
  • Fourier component analysis of diffraction features.
  • Patterson map analysis to recover phase information.

Main Results:

  • Identified limitations in early structural models and experimental data.
  • Proposed new structural models that better explain key diffraction features, such as specific 3/7th order beams.
  • Discovered new Si(111) 7 × 7 polymorphs with potential pi-bonding and magnetic surface states.
  • Revealed the Patterson map's utility in understanding lost phase information and favoring the DAS model historically.

Conclusions:

  • The widely accepted DAS model may not fully capture the complexity of the Si(111) 7 × 7 surface.
  • New structural models and polymorphs offer alternative explanations for diffraction data and suggest novel electronic/magnetic properties.
  • Advanced crystallographic methods provide deeper insights into surface structures and their underlying physics.