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All-Solid-State Lithium-Ion Batteries with Oxide/Sulfide Composite Electrolytes.

Young Seon Park1, Jae Min Lee1, Eun Jeong Yi1

  • 1Department of Materials Science & Engineering, Inha University, Incheon 22212, Korea.

Materials (Basel, Switzerland)
|April 30, 2021
PubMed
Summary

This study developed advanced solid-state electrolytes by combining LLZO and LPSC materials. These new composite electrolytes significantly boost ionic conductivity for better all-solid-state battery performance.

Keywords:
all-solid-state lithium-ion batteriesargyroditecomposite solid electrolytesgarnetlithium-ion conductivitysulfides

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Area of Science:

  • Materials Science
  • Electrochemistry
  • Solid-State Batteries

Background:

  • Solid-state electrolytes are crucial for next-generation batteries.
  • Lithium lanthanum zirconium oxide (LLZO) and lithium phosphorus sulfide chloride (LPSC) are promising solid electrolyte materials.
  • Achieving high ionic conductivity and good interfacial contact remains a challenge.

Purpose of the Study:

  • To fabricate and characterize Li6.3La3Zr1.65W0.35O12 (LLZO)-Li6PS5Cl (LPSC) composite electrolytes.
  • To investigate the effect of LPSC:LLZO ratio on microstructure, ionic conductivity, and electrochemical performance.
  • To evaluate the performance of all-solid-state cells (ASSCs) using these composite electrolytes.

Main Methods:

  • Fabrication of LLZO-LPSC composite electrolytes via room-temperature cold pressing.
  • Variation of LPSC:LLZO ratios (e.g., 7:3, 6:4).
  • Characterization of microstructure, ionic conductivity, and electrochemical performance in ASSCs with LiNi0.8Co0.1Mn0.1O2 (NCM811) cathodes.

Main Results:

  • Ionic conductivity of composite electrolytes was 3-4 orders of magnitude higher than pure LLZO.
  • High conductivity attributed to enhanced relative density and soft LPSC particles.
  • ASSCs with 7:3 and 6:4 LLZO:LPSC electrolytes achieved specific capacities of 163 and 167 mAh·g-1 at 0.1 C, respectively.

Conclusions:

  • LLZO-LPSC composite electrolytes offer significantly enhanced ionic conductivity.
  • Successful formation of good interfacial contact between NCM811 cathodes and composite electrolytes.
  • These composites show promise for high-performance all-solid-state batteries.