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Updated: Oct 7, 2026

High-pressure Sapphire Cell for Phase Equilibria Measurements of CO2/Organic/Water Systems
Published on: January 24, 2014
Sapphire optical viewport for high pressure and temperature applications
Till Ockenfels1, Frank Vewinger1, Martin Weitz1
1Institut für Angewandte Physik, Universität Bonn, Wegelerstr. 8, D-53115 Bonn, Germany.
Abstract:
We describe the design of a soldered sapphire optical viewport, which is useful for spectroscopic applications of samples at high temperatures and high pressures. The sapphire window is bonded via active soldering to a metal flange with a structure of two c-shaped rings made of different metallic materials in between, so as to mitigate thermally induced stress. A spectroscopic cell equipped with two of the optical viewports has been successfully operated with alkali metals in a noble gas environment at temperatures in the range of 20-450 °C at noble gas pressures from 10-6 mbar to 330 bars. In the upper pressure range, we observe a leakage rate smaller than our readout accuracy of 30 mbar per day.
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