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Comprehensive Compositional Analysis of Plant Cell Walls Lignocellulosic biomass Part II: Carbohydrates
Published on: March 12, 2010
Comparative hydrolysis analysis of cellulose samples and aspects of its application in conservation science
Manuel Becker1, Kyujin Ahn1,2, Markus Bacher1
1Department of Chemistry, Institute of Chemistry of Renewables, University of Natural Resources and Life Sciences, Muthgasse 18, Vienna, 1190 Austria.
Abstract:
Knowledge about the carbohydrate composition of pulp and paper samples is essential for their characterization, further processing, and understanding the properties. In this study, we compare sulfuric acid hydrolysis and acidic methanolysis, followed by GC-MS analysis of the corresponding products, by means of 42 cellulose and polysaccharide samples. Results are discussed and compared to solid-state NMR (crystallinity) and gel permeation chromatography (weight-averaged molecular mass) data. The use of the hydrolysis methods in the context of cellulose conservation science is evaluated, using e-beam treated and artificially aged cellulose samples.
Supplementary Information:
The online version contains supplementary material available at 10.1007/s10570-021-04048-6.
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