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Updated: Oct 25, 2025

Characterization, Quantification and Compound-specific Isotopic Analysis of Pyrogenic Carbon Using Benzene Polycarboxylic Acids BPCA
Published on: May 16, 2016
Characteristics of Impulse Carburization LPC Process.
Ryszard Filip1, Kamil Ochał1, Kamil Gancarczyk1
1Department of Materials Science, Faculty of Mechanical Engineering and Aeronautics, Rzeszow University of Technology, Powstancow Warszawy 12, 35-959 Rzeszow, Poland.
Impulse carburizing of Pyrowear53 steel created a 1200 µm layer with decreasing hardness and carbon content. Unique compressive stress peaks were observed due to dual martensite transformation fronts.
Area of Science:
- Materials Science
- Metallurgy
- Surface Engineering
Background:
- Pyrowear53 steel is a high-performance alloy used in demanding applications.
- Thermochemical treatments like carburizing are crucial for enhancing surface properties.
- Understanding the resulting microstructure and stress states is vital for predicting performance.
Purpose of the Study:
- To investigate the effects of impulse carburizing on Pyrowear53 steel.
- To analyze the resulting carburized layer's properties, including hardness, carbon content, and residual stresses.
- To elucidate the mechanisms behind the observed residual stress distribution.
Main Methods:
- Impulse carburizing (LPC) followed by quenching and tempering.
- Measurement of hardness, carbon content, and residual austenite.
- Analysis of residual stress profiles using appropriate techniques.
Main Results:
- Formation of a ~1200 µm thick carburized layer.
- Continuous gradient observed in hardness, carbon content, and residual austenite.
- A distinct zone of elevated compressive stresses found between 600-1000 µm depth.
Conclusions:
- The observed stress anomaly is attributed to two distinct martensite transformation fronts.
- This phenomenon is linked to the carbon content gradient and its effect on the martensite start temperature.
- The specific stress profile is characteristic of Pyrowear53 steel with 0.8-0.4 wt% carbon.
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