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Updated: Oct 25, 2025
Optimization of Processing of Tiebangchui with Highland Barley Wine Based on the Box-Behnken Design Combined with the Entropy Method
Published on: May 19, 2023
Effect of thermal processing on the molecular, structural, and antioxidant characteristics of highland barley
Yi-Peng Bai1, Hui-Ming Zhou1, Ke-Rui Zhu2
1State Key Laboratory of Food Science and Technology, Jiangnan University, Wuxi 214122, Jiangsu Province, PR China; School of Food Science and Technology, Jiangnan University, Wuxi 214122, Jiangsu Province, PR China.
Abstract:
This present work evaluated the effect of heat fluidization, microwave roasting and baking treatment of highland barley (HB) on the molecular, structural, thermal and antioxidant characteristics of β-glucan. Fluorescence microscopy results showed that heat fluidization exhibited the greatest disruption effect on endosperm cell walls, resulting in the highest extractability (3.35 ± 0.06 g/100 g flour) and purity (92.67 ± 0.73%) of β-glucan. After HB thermal processing, the molecular weight and polydispersity index of β-glucan were respectively reduced by 3.68%-90.35% and 26.45%-39.83%, and its microscopic molecular morphology transformed from large sphere aggregate to alveolate gel network structure. Meanwhile, the structural elucidation by X-ray diffraction and infrared spectroscopy revealed that thermal processing induced the scission of polymeric chain and formation of lattice-type microgels without changing the primary functional groups of β-glucan. Furthermore, thermogravimetry and antioxidant results indicated the thermal stability and antioxidant activity of β-glucan were enhanced by thermal processing.
