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Optimization of Pre-Heat Treatment for Nitriding
Matthias Steinbacher1,2, Stefanie Hoja1
1Leibniz-Institut für Werkstofforientierte Technologien-IWT, 28359 Bremen, Germany.
Materials (Basel, Switzerland)
|December 24, 2021
Summary
Optimizing pre-heat treatments for nitriding steels like EN31CrMoV9 and EN42CrMo4 enhances core strength and nitrided layer performance. Higher austenitization temperatures and bainitic microstructures significantly improve hardness and diffusion depth.
Area of Science:
- Materials Science and Engineering
- Metallurgy
- Surface Engineering
Background:
- Achieving adequate core strength in nitrided components is crucial for service life.
- Pre-heat treatment significantly influences the achievable strength of the nitrided layer.
- Optimizing pre-heat treatments can enhance the service characteristics of nitrided components.
Purpose of the Study:
- To investigate optimized pre-heat treatments for nitriding steels EN31CrMoV9 and EN42CrMo4 (AISI4140).
- To evaluate the impact of altered austenitization temperatures and bainitic microstructures on component properties.
- To determine methods for improving both core hardness and nitrided layer performance.
Main Methods:
- Investigated modified austenitization temperatures (e.g., 950 °C vs. 870 °C) for EN31CrMoV9 steel.
- Compared bainitic microstructures against conventional quenching and tempering treatments.
- Analyzed effects on carbide distribution, hardness, and diffusion depth in nitrided specimens.
Main Results:
- Increasing austenitization temperature for EN31CrMoV9 refined carbides and increased hardness.
- Bainitic microstructures resulted in greater diffusion depth and higher core hardness compared to quenched and tempered specimens.
- Subsequent nitriding tempered the bainite, leading to a reduction in its hardness.
Conclusions:
- Optimized pre-heat treatments, including higher austenitization temperatures and bainitic structures, offer significant improvements in nitrided steel properties.
- These treatments enhance core strength and nitrided layer characteristics, leading to better component performance.
- Further research may be needed to mitigate hardness loss in bainitic structures during nitriding.

