Adapting a continuous flow cryostat and a plate DAC to do high pressure Raman experiments at low temperatures

We present a method for modifying a continuous flow cryostat and a steel plate DAC (Diamond Anvil Cell) to perform high pressure micro-Raman experiments at low temperatures. Despite using a steel DAC with a lower specific heat capacity (∼335 J/kg K), this setup can routinely perform high pressure (∼10 GPa) measurements at temperatures as low as 26 K. This adaptation is appropriate for varying the temperature of the sample while keeping it at a constant pressure. We determined that the temperature variation across the sample chamber is about 1 K using both direct temperature measurements and finite element analysis of the heat transport across the DAC. We present Raman spectroscopy results on elemental selenium at high pressures and low temperatures using our modified setup.