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Updated: Oct 8, 2025
Synthesis and Characterization of Functionalized Metal-organic Frameworks
Published on: September 5, 2014
Significance of an Environmental Gas Cell to Obtain a Fully Dehydrated Form and CO2-Pressurized Structure of a
Prem Lama1,2, Ashutosh Rawat1, Phumile Sikiti3
1DHOP Division, Council of Scientific and Industrial Research, Indian Institute of Petroleum, Haridwar Road, Mohkampur, Dehradun 248005, India.
Abstract:
The single-crystal X-ray diffraction method was employed to characterize a rigid hydrated metal-organic framework (MOF), [Co2(MA)(INA)·2H2O], that displays an affinity toward water molecules under ambient conditions after dehydration. The fully dehydrated form was obtained using an environmental gas cell technique in a stepwise manner followed by its CO2-pressurized structure at 298 K using in situ crystallography.
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