Jove
Visualize
Contact Us
JoVE
x logofacebook logolinkedin logoyoutube logo
ABOUT JoVE
OverviewLeadershipBlogJoVE Help Center
AUTHORS
Publishing ProcessEditorial BoardScope & PoliciesPeer ReviewFAQSubmit
LIBRARIANS
TestimonialsSubscriptionsAccessResourcesLibrary Advisory BoardFAQ
RESEARCH
JoVE JournalMethods CollectionsJoVE Encyclopedia of ExperimentsArchive
EDUCATION
JoVE CoreJoVE BusinessJoVE Science EducationJoVE Lab ManualFaculty Resource CenterFaculty Site
Terms & Conditions of Use
Privacy Policy
Policies

Related Concept Videos

Electrodeposition01:08

Electrodeposition

740
Electrodeposition is a technique used to separate an analyte from interferents by electrochemical processes. Here, the analyte is a metal ion that can be deposited on an electrode immersed in the sample solution. The electrochemical setup consists of an anode and a cathode. When an electric current is applied to the setup, oxidation occurs at the anode. At the cathode, which consists of a large metal surface, metal ions undergo reduction and deposit onto the surface.
Electrodeposition can...
740
Batteries and Fuel Cells03:12

Batteries and Fuel Cells

28.1K
A battery is a galvanic cell that is used as a source of electrical power for specific applications. Modern batteries exist in a multitude of forms to accommodate various applications, from tiny button batteries such as those that power wristwatches to the very large batteries used to supply backup energy to municipal power grids. Some batteries are designed for single-use applications and cannot be recharged (primary cells), while others are based on conveniently reversible cell reactions that...
28.1K

You might also read

Related Articles

Articles linked to this work by shared authors, journal, and citation graph.

Sort by
Same author

Toward Achieving a High Ionic Conducting Halide Solid Electrolyte through Low-Cost Metal (Zr and Fe) and F Substitution and Their Admirable Performance in All-Solid-State Batteries.

ACS applied materials & interfaces·2024
Same author

LiNi<sub>0.6</sub>Co<sub>0.2</sub>Mn<sub>0.2</sub>O<sub>2</sub> Cathode-Solid Electrolyte Interfacial Behavior Characterization Using Novel Method Adopting Microcavity Electrode.

Molecules (Basel, Switzerland)·2023
Same author

Preparation of Metal-Oxide-Doped Li<sub>7</sub>P<sub>2</sub>S<sub>8</sub>Br<sub>0.25</sub>I<sub>0.75</sub> Solid Electrolytes for All-Solid-State Lithium Batteries.

ACS applied materials & interfaces·2023
Same author

FeS-biochar and Zn(0)-biochar for remediation of redox-reactive contaminants.

RSC advances·2022
Same author

NiCo<sub>2</sub>S<sub>4</sub> Bi-metal Sulfide Coating on LiNi<sub>0.6</sub>Co<sub>0.2</sub>Mn<sub>0.2</sub>O<sub>2</sub> Cathode for High-Performance All-Solid-State Lithium Batteries.

ACS omega·2021
Same author

Facile hydrothermal synthesis and characterization of Co<sub>2</sub>GeO<sub>4</sub>/r-GO@C ternary nanocomposite as negative electrode for Li-ion batteries.

Journal of colloid and interface science·2017

Related Experiment Video

Updated: Sep 25, 2025

Solid-state Graft Copolymer Electrolytes for Lithium Battery Applications
05:33

Solid-state Graft Copolymer Electrolytes for Lithium Battery Applications

Published on: August 12, 2013

21.8K

Improving the electrochemical performance of cathode composites using different sized solid electrolytes for all

Rajesh Rajagopal1,2, Yuvaraj Subramanian1, Kwang-Sun Ryu1,2

  • 1Department of Chemistry, University of Ulsan Doowang-dong, Nam-gu Ulsan 44776 Korea ryuks@ulsan.ac.kr +82-52-712-8002 +82-52-712-8003.

RSC Advances
|May 2, 2022
PubMed
Summary

Mixed particle-sized sulfide solid electrolytes enhance all-solid-state lithium battery performance. These composites show improved specific capacitance compared to uniform-sized electrolytes, demonstrating superior electrochemical properties.

More Related Videos

Screening of Coatings for an All-Solid-State Battery Using In Situ Transmission Electron Microscopy
07:20

Screening of Coatings for an All-Solid-State Battery Using In Situ Transmission Electron Microscopy

Published on: January 20, 2023

2.7K
Characterization of Electrode Materials for Lithium Ion and Sodium Ion Batteries Using Synchrotron Radiation Techniques
10:03

Characterization of Electrode Materials for Lithium Ion and Sodium Ion Batteries Using Synchrotron Radiation Techniques

Published on: November 11, 2013

25.6K

Related Experiment Videos

Last Updated: Sep 25, 2025

Solid-state Graft Copolymer Electrolytes for Lithium Battery Applications
05:33

Solid-state Graft Copolymer Electrolytes for Lithium Battery Applications

Published on: August 12, 2013

21.8K
Screening of Coatings for an All-Solid-State Battery Using In Situ Transmission Electron Microscopy
07:20

Screening of Coatings for an All-Solid-State Battery Using In Situ Transmission Electron Microscopy

Published on: January 20, 2023

2.7K
Characterization of Electrode Materials for Lithium Ion and Sodium Ion Batteries Using Synchrotron Radiation Techniques
10:03

Characterization of Electrode Materials for Lithium Ion and Sodium Ion Batteries Using Synchrotron Radiation Techniques

Published on: November 11, 2013

25.6K

Area of Science:

  • Materials Science
  • Electrochemistry
  • Solid-State Chemistry

Background:

  • Sulfide solid electrolytes are promising for all-solid-state lithium batteries due to their high ionic conductivity.
  • Optimizing the particle size distribution of solid electrolytes is crucial for improving interfacial contact and overall battery performance.
  • Previous studies have focused on uniform particle sizes, leaving the effect of mixed sizes underexplored.

Purpose of the Study:

  • To investigate the impact of different particle-sized Li7P2S8I sulfide solid electrolytes on the electrochemical performance of LiNi0.8Co0.1Mn0.1O2 (NCM 811) cathode composites.
  • To compare the performance of all-solid-state lithium batteries fabricated with mixed particle-sized versus uniform particle-sized solid electrolytes.
  • To understand the relationship between particle size distribution and ionic conductivity in sulfide solid electrolytes.

Main Methods:

  • Preparation of Li7P2S8I solid electrolytes with varying particle sizes using high energy ball milling and solution methods.
  • Characterization of solid electrolytes using powder X-ray diffraction (PXRD) for structural analysis and field emission electron microscopy (FESEM) for surface morphology and particle size.
  • Measurement of ionic conductivity via electrochemical impedance spectroscopy (EIS).
  • Fabrication and electrochemical performance testing of all-solid-state lithium batteries utilizing NCM 811 cathodes with different solid electrolyte particle sizes.

Main Results:

  • Sulfide solid electrolytes with mixed particle sizes were successfully prepared and characterized.
  • Electrochemical impedance spectroscopy confirmed differences in ionic conductivity based on particle size distribution.
  • All-solid-state lithium batteries employing mixed particle-sized solid electrolyte cathode composites demonstrated higher specific capacitance (127.2 mA h g-1) compared to those with uniform-sized electrolytes (117.1 mA h g-1).

Conclusions:

  • Mixed particle-sized sulfide solid electrolytes significantly improve the electrochemical performance of NCM 811 based all-solid-state lithium batteries.
  • The enhanced performance is attributed to optimized interfacial contact and ion transport facilitated by the mixed particle size distribution.
  • This study highlights the importance of particle size engineering in developing high-performance solid-state batteries.