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Continuous syntheses of carbon-supported Pd and Pd@Pt core-shell nanoparticles using a flow-type single-mode
Masato Miyakawa1, Norihito Hiyoshi1, Hidekazu Koda2
1National Institute of Advanced Industrial Science and Technology, AIST 4-2-1, Nigatake, Miyagino-ku Sendai 983-8551 Japan masato-miyakawa@aist.go.jp m-nishioka@aist.go.jp.
Abstract:
Continuous syntheses of carbon-supported Pd@Pt core-shell nanoparticles were performed using microwave-assisted flow reaction in polyol to synthesize carbon-supported core Pd with subsequent direct coating of a Pt shell. By optimizing the amount of NaOH, almost all Pt precursors contributed to shell formation without specific chemicals.
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