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Published on: December 6, 2021
Microwave-assisted synthesis of mutually embedded Rh concave nanocubes with enhanced electrocatalytic activity
Junxuan Xu1, Hongbin Tang1, Baogui Ning1
1College of Chemistry and Material Science, South-Central University for Nationalities Wuhan 430074 China huangt208@163.com.
Abstract:
Novel mutually embedded Rh concave nanocubes were synthesized by reducing Rh(acac)3 in tetraethylene glycol in the presence of benzyldimethylhexadecylammonium, KI and polyvinylpyrrolidone under microwave irradiation for 120 s. KI and HDBAC were crucial to the formation of mutually embedded nanostructures. The as-prepared Rh nanocrystals exhibited higher electrocatalytic activity and stability.

