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Updated: Sep 6, 2025

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Processing of Bulk Nanocrystalline Metals at the US Army Research Laboratory
Published on: March 7, 2018
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Implications of Microstructure in Helium-Implanted Nanocrystalline Metals.
James E Nathaniel1,2, Osman El-Atwani1,3, Shu Huang4
1Department of Materials Science & Engineering, Drexel University, Philadelphia, PA 19104, USA.
Materials (Basel, Switzerland)
|June 24, 2022
Summary
Nanocrystalline nickel (Ni) and iron (Fe) metals resist helium bubble formation differently. NC Ni shows superior resistance to irradiation-induced bubble growth compared to NC Fe, indicating its potential for extreme environments.
Area of Science:
- Materials Science
- Nuclear Engineering
- Nanotechnology
Background:
- Helium bubbles form in nuclear reactor materials due to radiation damage, causing swelling and embrittlement.
- Nanocrystalline (NC) metals are promising for radiation resistance due to high defect sink densities.
- Mechanisms of defect evolution in NC metals under extreme conditions require further investigation.
Purpose of the Study:
- To investigate the performance of NC nickel (Ni) and iron (Fe) under helium bombardment.
- To understand the mechanisms of helium bubble formation and evolution in NC metals.
- To compare the radiation resistance of NC Ni and NC Fe.
Main Methods:
- Helium bombardment of NC Ni and Fe specimens.
- Transmission electron microscopy (TEM) for bubble density analysis.
- Rate theory modeling to study helium diffusion and trapping kinetics.
Main Results:
- Bubble density increased with saturation in both NC Ni and Fe.
- Fe exhibited over 300% greater bubble density than Ni.
- Helium is preferentially trapped in NC Fe grains, while it migrates to grain boundaries in NC Ni.
Conclusions:
- Grain boundaries significantly influence bubble swelling and can dominate over crystal structure.
- NC Ni demonstrates superior resistance to helium bubble growth compared to NC Fe.
- NC Ni shows high potential for applications in extreme environments susceptible to helium bubble formation.

