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Dual modification of cellulose with esterification and carbonation in DMSO/DBU/CO2 system as fluorescent additive for
Jiangqin Lu1, Shan Lu2, Qinghua Cao2
1Key Laboratory of Bio-Based Polymeric Materials of Zhejiang Province, Ningbo Institute of Materials Technology and Engineering, Chinese Academy of Sciences, Ningbo, Zhejiang, 315201, China; Nano Science and Technology Institute, University of Science and Technology of China, Suzhou, Jiangsu, 230026, China.
Abstract:
An easy and effective way to synthesize dual-functionalized cellulose derivatives with processability and fluorescence functionality by one-pot modification of successive esterification and carbonation under mild condition is established with the use of DMSO/DBU/CO2 system. Accordingly, four kinds of dual-functionalized cellulose derivatives with rather good fluorescent response are obtained. After blending the synthesized dual-functionalized cellulose derivative with cellulose acetate as functional additive in solution, cast film with the elastic modulus, stress and strain reaches to 2.2 GPa, 34.1 MPa and 5.7% is prepared. Besides, the cast film also exhibits the ability to detect the pH value at 12-14 with detection accuracy of 0.4 through the change of fluorescent color. This research shows a simple but effective way to prepare dual-functionalized cellulose derivatives for the high-quality applications in field of detection.
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