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Gordon Coupler with Inductive or Capacitive Iris for Small EPR Resonators for Aqueous Samples
Richard R Mett1,2, James S Hyde1
1National Biomedical EPR Center, Department of Biophysics, Medical College of Wisconsin, 8701 Watertown Plank Road, Milwaukee, WI 53226, USA.
Applied Magnetic Resonance
|August 22, 2022
Summary
This study extends the Gordon coupler for Electron Paramagnetic Resonance (EPR) experiments, enabling efficient microwave power delivery to X-band resonators using various dielectrics. The enhanced design reduces frequency pulling for improved EPR spectroscopy.
Area of Science:
- Physics
- Spectroscopy
- Materials Science
Background:
- The Gordon coupler, initially for Electron Paramagnetic Resonance (EPR) at liquid helium temperatures, couples microwave power to resonators via an evanescent wave.
- Previous extensions adapted the coupler for cavity and loop-gap resonators, using low-dielectric plastics like Teflon for aqueous samples.
- Microphonics from helium bubbling were a challenge in early applications.
Purpose of the Study:
- To extend the Gordon coupler's application to X-band five-loop-four-gap resonators.
- To investigate the use of fused quartz, sapphire, and rutile as dielectric materials.
- To optimize power matching and minimize resonant frequency shifts using a capacitive iris.
Main Methods:
- Adaptation of the Gordon coupler design for X-band dielectric resonators.
- Utilization of fused quartz, sapphire, and rutile dielectrics.
- Finite element modeling (FEM) for electromagnetic field analysis.
- Integration of a capacitive iris for improved resonator matching.
Main Results:
- The Gordon coupler was successfully adapted for X-band five-loop-four-gap resonators with new dielectric materials.
- FEM confirmed the electromagnetic field behavior and the coupler's scalability with dielectric resonator dimensions.
- The capacitive iris effectively reduced resonant frequency pulling during power matching.
Conclusions:
- The extended Gordon coupler provides a versatile and efficient method for microwave power delivery in advanced EPR resonator systems.
- The use of robust dielectric materials like quartz, sapphire, and rutile expands the operational temperature and sample compatibility.
- This advancement facilitates high-performance EPR spectroscopy with improved signal-to-noise ratios and stability.

