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Solid-state Graft Copolymer Electrolytes for Lithium Battery Applications
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3D Printing Nanostructured Solid Polymer Electrolytes with High Modulus and Conductivity.

Kenny Lee1, Yuan Shang2,3, Valentin A Bobrin1

  • 1Cluster for Advanced Macromolecular Design (CAMD), UNSW Australia, Sydney, NSW, 2052, Australia.

Advanced Materials (Deerfield Beach, Fla.)
|August 25, 2022
PubMed
Summary
This summary is machine-generated.

Researchers developed a 3D-printed solid polymer electrolyte using a novel microphase-separation method. This scalable manufacturing process yields high-performance materials for advanced energy storage, offering both ionic conductivity and mechanical strength.

Keywords:
3D printingand nanostructured materialsnanostructured materialsphotoreversible addition-fragmentation chain transfer (photoRAFT) polymerizationpolymerization-induced microphase separation (PIMS)solid polymer electrolytes (SPEs)

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Area of Science:

  • Materials Science
  • Electrochemistry
  • Polymer Chemistry

Background:

  • Advanced solid-state energy storage requires scalable, high-modulus solid-state electrolytes.
  • Existing electrolytes often struggle to balance high ionic conductivity with robust mechanical integrity.
  • Manufacturing challenges limit the widespread adoption of high-performance solid electrolytes.

Purpose of the Study:

  • To develop an efficient, one-step manufacturing process for solid polymer electrolytes.
  • To create materials with nanoscale ion-conducting channels within a rigid polymer matrix.
  • To demonstrate the application of these electrolytes in energy storage devices.

Main Methods:

  • Utilized Digital Light Processing (DLP) 3D printing for fabrication.
  • Employed a visible-light-mediated polymerization-induced microphase-separation approach.
  • Incorporated poly(ethylene oxide) domains swollen with ionic liquid within a crosslinked polymer matrix.

Main Results:

  • Achieved solid polymer electrolytes with nanoscale, tunable architectures.
  • Obtained outstanding room-temperature shear modulus (G' > 10^8 Pa).
  • Reached high ionic conductivities up to σ = 3 × 10^-4 S cm^-1.
  • Demonstrated functionality in a symmetric carbon supercapacitor.

Conclusions:

  • The developed 3D printing method enables on-demand manufacturing of custom-geometry solid polymer electrolytes.
  • The materials exhibit excellent mechanical properties and ionic conductivity, suitable for energy storage.
  • This approach offers a scalable and cost-effective solution for producing advanced solid electrolytes.