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Updated: Jun 25, 2026

Protocol of Electrochemical Test and Characterization of Aprotic Li-O2 Battery
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Co3O4-MoSe2@C nanocomposite as a multi-functional catalyst for electrochemical water splitting and lithium-oxygen
Wenjing Yu1, Shaohua Zhang1, Kun Gao1
1Beijing Key Laboratory of Photoelectronic/Electrophotonic Conversion Materials, Key Laboratory of Cluster Science, Ministry of Education, School of Chemistry and Chemical Engineering, Beijing Institute of Technology, Beijing 100081, People's Republic of China.
Abstract:
Co3O4-MoSe2@C nanocomposite has been prepared by a convenient method via combining hydrothermally synthesized MoSe2@C and Co3O4. When catalyzing the hydrogen evolution reaction and oxygen evolution reaction, the catalyst features low overpotentials of 144 mV and 360 mV (both at 10 mA cm-2current density), respectively. It can also serve as the cathode in the lithium-oxygen battery and the device shows a low charging-discharging overpotential of 1.50 V with a stable performance of over 200 cycles at current density of 1000 mA g-1, shedding light on the design and synthesis of novel multifunctional electrocatalysts for energy conversions.
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