An integrated process using acetic acid hydrolysis and deep eutectic solvent pretreatment for xylooligosaccharides...

Organic acid hydrolysis for xylooligosaccharides (XOS) production from lignocelluloses provides the benefits of simple operation, rapid reaction and high XOS yield. However, no literature reported the XOS production from wheat bran (WB) by organic acid hydrolysis. In this paper, acetic acid (AA) hydrolysis was employed to produce XOS from WB. After AA hydrolysis (5 %, v/v, 170 °C, 20 min) of 100 g/L WB, the concentrations of X2, X3, X4, X5 and X6 were 2.4, 5.0, 1.9, 1.9 and 1.4 g/L respectively and the total XOS yield was 62.9 %, which was the highest among the previous researches. The arabinose yield reached 76.1 %. Then, AA-hydrolyzed WB was delignified by deep eutectic solvent (DES) pretreatment and the resulting residue had the glucose and xylose yields of 83.8 % and 54.8 %, respectively. This work offers a productive method for the conversion of WB into XOS, arabinose and glucose by AA hydrolysis and DES pretreatment.