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Updated: Aug 28, 2025
Preparation of Liquid-exfoliated Transition Metal Dichalcogenide Nanosheets with Controlled Size and Thickness: A State of the Art Protocol
Published on: December 20, 2016
Rapid synthesis of defective and composition-controlled metal chalcogenide nanosheets by supercritical hydrothermal
Yuta Nakayasu1, Siobhan Bradley2, Hiroaki Kobayashi1
1IMRAM, Tohoku University 2-1-1 Katahira, Aoba-ku Sendai Miyagi 980-8577 Japan nakayasu@tohoku.ac.jp itaru.homma.e8@tohoku.ac.jp +81 22(217)5828 +81 22(217)5816.
Abstract:
This study presents a simple one-pot synthesis method to achieve few-layered and defective Mo(S,Se)2 and (Mo,W)S2 by using supercritical water with organic reducing agents from simple and less-toxic precursors. This synthesis process is expected to be suitable for preparing other various kinds of TMD solid solutions.
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