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Preliminary study on forgery identification of Hetian Jade with Instrumental Neutron Activation Analysis
Krishnakumar Nangeelil1, Peter Dimpfl1, Mayir Mamtimin2
1Department of Health Physics and Diagnostic Sciences, University of Nevada Las Vegas, Las Vegas, NV, 89154, USA.
Instrumental Neutron Activation Analysis (INAA) effectively identified genuine Hetian Jade from counterfeits by analyzing elemental compositions. This method, aided by principal component analysis (PCA), offers high sensitivity for geological sample analysis.
Area of Science:
- Geochemistry
- Analytical Chemistry
- Materials Science
Background:
- Hetian Jade is a valuable gemstone with a significant market.
- Distinguishing genuine Hetian Jade from counterfeits is economically important.
- Elemental analysis provides a basis for material identification.
Purpose of the Study:
- To apply Instrumental Neutron Activation Analysis (INAA) for elemental analysis of geological samples.
- To differentiate genuine Hetian Jade from counterfeit samples using INAA.
- To explore the utility of chemometric techniques in conjunction with INAA for jade authentication.
Main Methods:
- Instrumental Neutron Activation Analysis (INAA) was performed on geological samples.
- Samples included genuine Hetian Jade, counterfeit jade, and local granitoid rocks.
- Chemometric techniques, specifically Principal Component Analysis (PCA), were employed for data analysis.
Main Results:
- INAA successfully provided multi-elemental concentration data for all analyzed samples.
- Distinct elemental profiles were observed between genuine Hetian Jade and counterfeit samples.
- PCA effectively visualized the separation of sample groups based on elemental composition.
Conclusions:
- INAA is a highly sensitive technique for determining elemental concentrations in geological materials.
- INAA, combined with PCA, provides a robust method for authenticating Hetian Jade.
- This approach can reliably distinguish genuine Hetian Jade from imitations based on elemental fingerprinting.
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