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Torrefaction characteristics of cellulose loaded with boric acid
Zhiguang Yang1, Yaochao Zhang2, Xinfeng Zhu2
1Henan Province Key Laboratory of Water Pollution Control and Rehabilitation Technology, Henan University of Urban Construction, Pingdingshan, 467036, China; College of Resources and Environment, Chinese Academy of Sciences, Beijing, 100085, China.
Abstract:
To explore the catalytic effect of boric acid on biomass, cellulose loaded with boric acid was roasted by a tubular furnace. The gaseous products were adsorbed by activated carbon and then analyzed by GC-MS. Boric acid was shown to improve the selectivity of the product levoglucosenone (LGO). The effects of the parameters such as boric acid loading, nitrogen flow, and temperature on the torrefaction behavior of cellulose were investigated. In the studied temperature range of 240-420 °C, the yield of LGO first increases and then decreases. In addition, its yield increases directly with increasing nitrogen flow rate. The results show that the highest LGO yield of 6.64% (analytical value) can be obtained under 10% (w/w) boric acid loading, 380 °C and nitrogen flow rate of 65 ml/min conditions.
