Related Experiment Video
Updated: Aug 19, 2025

09:46
Synthesis of Plant Phenol-derived Polymeric Dyes for Direct or Mordant-based Hair Dyeing
Published on: December 1, 2016
9.3K
Pectin-based color indicator films incorporated with spray-dried Hibiscus extract microparticles
Juliana Farinassi Mendes1, Laís Bruno Norcino2, Anny Manrich1
1National Laboratory of Nanotechnology for Agriculture (LNNA), Embrapa Instrumentation, São Carlos 13560-970, SP, Brazil.
Food Research International (Ottawa, Ont.)
|December 3, 2022
Summary
New pH-sensing colorimetric films use hibiscus extract microparticles in pectin (HM) films for food freshness monitoring. These smart films change color with pH, offering a natural indicator for smart packaging applications.
Area of Science:
- Food Science
- Materials Science
- Polymer Science
Background:
- Anthocyanin-based colorimetric films are gaining interest for freshness monitoring.
- Developing natural pH indicators for smart packaging is crucial for food safety.
Purpose of the Study:
- To develop pH-sensing colorimetric films using pectin (HM) and aqueous hibiscus extract (HAE) microparticles.
- To evaluate the physicochemical, morphological, thermal, barrier, and antioxidant properties of these films.
- To assess the color change response of the films to different pH levels.
Main Methods:
- Aqueous hibiscus extract (HAE) microparticles were produced via spray drying using inulin (IN) and maltodextrin (MD) as wall materials.
- Pectin (HM)-based films incorporating HAE microparticles were fabricated using continuous casting.
- Films were characterized for mechanical, thermal, barrier (WVTR), antioxidant, and colorimetric properties.
Main Results:
- HAE microparticle incorporation modified pectin film properties, including mechanical behavior and barrier characteristics (11-22% WVTR reduction).
- Improved thermal stability was observed in the pectin films with HAE microparticles.
- The color of the developed smart films demonstrated a clear pH-dependent variation.
Conclusions:
- The developed pectin-based films with hibiscus extract microparticles function as effective natural pH indicators.
- These smart films exhibit unique features suitable for application in smart packaging systems for freshness monitoring.

