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Functionalized Soybean Oil- and Vanillin-Based Dual Cure Photopolymerizable System for Light-Based 3D Structuring.

Vilte Sereikaite1, Aukse Navaruckiene1, Justinas Jaras1

  • 1Department of Polymer Chemistry and Technology, Kaunas University of Technology, Radvilenu Rd. 19, LT-50254 Kaunas, Lithuania.

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|December 23, 2022
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Summary
This summary is machine-generated.

Researchers developed a stable, plant-derived dual cure photopolymerizable resin. This novel material exhibits rapid photocuring, enhanced mechanical properties, and thermal stability, outperforming existing vanillin-based polymers.

Keywords:
acrylated epoxidized soybean oildual-curingmultiphoton polymerizationphotocross-linkingstereolithographytwo-beam initiation thresholdvanillin dimethacrylate

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Area of Science:

  • Polymer Chemistry
  • Materials Science
  • Biomaterials

Background:

  • Developing stable and high-performance photopolymerizable resins is crucial for advanced applications.
  • Existing systems often face challenges with premature polymerization and limited mechanical properties.
  • Plant-derived monomers offer a sustainable alternative for polymer synthesis.

Purpose of the Study:

  • To develop a novel dual cure photopolymerizable system using plant-derived monomers.
  • To overcome stability and premature polymerization issues in vanillin-based resins.
  • To enhance mechanical properties and thermal stability for improved performance.

Main Methods:

  • Combining acrylated epoxidized soybean oil, vanillin dimethacrylate, and pentaerythritol tetrakis (3-mercaptopropionate).
  • Optimizing resin composition for stability and selective polymerization.
  • Characterizing photocuring kinetics, mechanical properties (rigidity, Young's modulus, compression modulus), and thermal stability (TGA).
  • Applying the system in stereolithography and measuring the two-beam initiation threshold.

Main Results:

  • Achieved a stable resin with a six-month shelf life at 4 °C.
  • Demonstrated rapid photocuring without an induction period.
  • Obtained significantly improved mechanical properties: rigidity (317.66 MPa), Young's modulus (4753 MPa), and compression modulus (1634 MPa).
  • Exhibited high thermal stability with a 10% weight loss temperature of 373 °C.
  • Successfully applied in stereolithography and characterized polymerization threshold.

Conclusions:

  • The developed dual cure system offers superior stability and mechanical performance compared to existing vanillin-based polymers.
  • The plant-derived monomers provide a sustainable route to high-performance photopolymers.
  • The controlled polymerization threshold offers potential for cost-effective and reliable 3D printing workstations.