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Updated: Aug 16, 2025

Characterization of Ultra-fine Grained and Nanocrystalline Materials Using Transmission Kikuchi Diffraction
Published on: April 1, 2017
Granular crystals as strong and fully dense architectured materials.
Ashta Navdeep Karuriya1, Francois Barthelat1
1Department of Mechanical Engineering, University of Colorado, Boulder, CO 80309.
Researchers created strong, recyclable 3D architectured materials using vibration-assembled granular crystals. These materials exhibit unique plasticity and strength, offering potential for advanced engineering applications.
Area of Science:
- Materials Science
- Mechanical Engineering
- Solid Mechanics
Background:
- Dense topologically interlocked panels utilize stiff building blocks with frictional contact for enhanced mechanical properties.
- Existing strategies focus on panels, limiting applications for bulk materials.
Purpose of the Study:
- To extend the concept of topologically interlocked structures to fully dense, 3D architectured materials using space-filling grains.
- To investigate the mechanical behavior and deformation mechanisms of these novel granular crystals.
Main Methods:
- 3D printing of rhombic dodecahedral and truncated octahedral grains.
- Assembly of grains into face-centered cubic and body-centered cubic granular crystals using mechanical vibrations.
- Triaxial compression testing to evaluate mechanical performance and deformation mechanisms.
- Development of a three-length scale theoretical model to capture observed phenomena.
Main Results:
- Granular crystals demonstrated up to 25 times greater strength than randomly packed spheres.
- Materials exhibited nonlinear deformations, crystal plasticity, geometrical hardening, shear-induced dilatancy, and microbuckling.
- A novel pressure-dependent granular crystal plasticity with interlocked slip planes was observed, forbidding slip in certain directions.
- Recycling of tested grains showed no loss of material strength.
Conclusions:
- The study successfully created robust 3D architectured materials with exceptional strength and damage tolerance through controlled grain assembly.
- Observed unique deformation mechanisms, including granular crystal plasticity, offer new avenues for material design.
- These materials show potential for advanced applications requiring high performance, repairability, and recyclability.
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