Protocol for quantitative nuclear magnetic resonance for deciphering electrolyte decomposition reactions in
Ming-Yue Zhou1, Xiao-Qing Ding2, Li-Peng Hou1
1Beijing Key Laboratory of Green Chemical Reaction Engineering and Technology, Department of Chemical Engineering, Tsinghua University, Beijing 100084, China.
Abstract:
In this protocol, we describe the quantification of electrolytes using nuclear magnetic resonance. We detail the steps involved for battery cycling, sample preparation, instrument operation, and data analysis. The protocol can be used to quantify electrolyte decomposition reactions and the apparent electron transfer numbers of different electrolyte components. The protocol is optimized for lithium-based anode-free batteries but can also be applied to other rechargeable batteries. For complete details on the use and execution of this protocol, please refer to Zhou et al. (2022).1.
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