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Updated: Aug 14, 2025
Fabrication of Large-area Free-standing Ultrathin Polymer Films
Published on: June 3, 2015
Protocol for the synthesis and use of U selective hydrogen-bonded organic framework to prepare large-area
Karan Marvaniya1, Ashish Maurya1, Priyanka Dobariya1
1CSIR-Central Salt and Marine Chemicals Research Institute, Bhavnagar 364002, India; Academy of Scientific and Innovative Research (AcSIR), CSIR-Human Resource Development Centre, (CSIR-HRDC) Campus, Sector 19, Kamla Nehru Nagar, Ghaziabad 201002, India.
Abstract:
Hydrogen-bonded organic frameworks (HOFs) are assembled via non-covalent secondary interactions that are scintillating examples of porous crystalline materials. This protocol highlights the synthesis and characterization of U selective, permanently porous, hydrolytically stable single-component CSMCRIHOF-1. We describe the steps to synthesize hydrogen bonding motif and single crystals of CSMCRIHOF-1. We then detail the preparation of large-area free-standing thin film of CSMCRIHOF-1 (TFCH). Finally, we describe the assessment of the hydrolytic stability of CSMCRIHOF-1 and TFCH. For complete details on the use and execution of this protocol, please refer to Kaushik et al. (2022).1.
