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Updated: Aug 5, 2025

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Sample Preparation and Experimental Design for In Situ Multi-Beam Transmission Electron Microscopy Irradiation Experiments
Published on: June 27, 2022
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Microstructural Effects on Irradiation Creep of Reactor Core Materials
Malcolm Griffiths1,2,3
1Department of Mechanical & Aerospace Engineering, Carleton University, Ottawa, ON K1S5B6, Canada.
Materials (Basel, Switzerland)
|March 29, 2023
Summary
Irradiation creep in nuclear materials is driven by temperature and defect production, influencing microstructure and mass transport. Diffusional mass transport dominates Zr-alloys below 300°C, with grain structure being key.
Area of Science:
- Materials Science
- Nuclear Engineering
- Physics
Background:
- Irradiation creep is crucial for nuclear reactor core materials.
- Experimental study of irradiation creep is challenging, leading to various theoretical models.
- Microstructure significantly influences irradiation creep mechanisms and mass transport.
Purpose of the Study:
- To describe and discuss microstructurally dependent irradiation creep mechanisms and models.
- To develop and validate a rate theory model for creep in Zr-2.5Nb pressure tubing.
- To determine dominant creep mechanisms and microstructural parameters for Zr-alloys and austenitic alloys.
Main Methods:
- Development of a rate theory model incorporating as-fabricated microstructure.
- Comparison of model predictions with experimental measurements for Zr-2.5Nb tubes.
- Analysis of microstructural dependencies for Zr-alloys and austenitic alloys.
Main Results:
- The developed rate theory model shows good agreement with experimental data for Zr-2.5Nb pressure tubing.
- Diffusional mass transport is identified as the dominant creep mechanism for Zr-alloys at temperatures < 300 °C and stresses < 150 MPa.
- Grain structure is the most critical microstructural parameter for irradiation creep in Zr-alloys under these conditions.
Conclusions:
- Diffusional mass transport is the primary mechanism for Zr-alloys under specific temperature and stress conditions.
- Grain structure is the most significant microstructural factor controlling irradiation creep in Zr-alloys.
- Austenitic alloys exhibit similar microstructural dependencies but extend to higher temperature and stress ranges, with dislocation slip dominating at low temperatures (< 100 °C).
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