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Microstructural Characterization of Al/CNTs Nanocomposites after Cold Rolling
Íris Carneiro1,2,3, José V Fernandes4, Sónia Simões1,2
1DEMM-Department of Metallurgical and Materials Engineering, University of Porto, Rua Dr. Roberto Frias, 4200-465 Porto, Portugal.
Nanomaterials (Basel, Switzerland)
|April 28, 2023
Summary
This study investigated aluminium-carbon nanotube (Al/CNTs) nanocomposite deformation during cold rolling. Powder metallurgy followed by cold rolling reliably enhances microstructure and mechanical properties, with CNTs influencing grain behavior and texture evolution.
Area of Science:
- Materials Science
- Mechanical Engineering
- Nanotechnology
Background:
- Metal matrix nanocomposites, particularly Al/CNTs, offer potential for advanced components in the mobility industry.
- Powder metallurgy is a key production process for these nanocomposites, necessitating research into their deformation behavior.
- Understanding deformation is crucial for optimizing microstructure and mechanical properties by reducing porosity.
Purpose of the Study:
- To investigate the deformation behavior of Al/CNTs nanocomposites during cold rolling.
- To evaluate the reliability of the powder metallurgy route followed by cold rolling for Al/CNTs nanocomposites.
- To analyze the influence of CNTs on microstructure, crystallographic orientation, and mechanical properties.
Main Methods:
- Production of Al/CNTs nanocomposites via powder metallurgy.
- Microstructural characterization using optical microscopy (OM), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and electron backscattered diffraction (EBSD).
- Mechanical characterization including hardness and tensile strength testing during cold rolling.
Main Results:
- The powder metallurgy route combined with cold rolling is effective for Al/CNTs nanocomposites.
- Microstructural analysis revealed distinct crystallographic orientations in nanocomposites compared to the Al matrix.
- CNTs influence grain rotation during sintering and deformation, leading to different texture evolution and an initial decrease in hardness and strength due to the Bauschinger effect.
Conclusions:
- Cold rolling of powder metallurgy-produced Al/CNTs nanocomposites is a viable method for property enhancement.
- The presence of CNTs significantly alters the crystallographic texture and deformation mechanisms.
- Differences in texture evolution between Al/CNTs nanocomposites and the Al matrix account for variations in mechanical properties during cold rolling.

