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Published on: May 21, 2019
Protocol for photoelectrocatalytic synthesis of aromatic azo compounds from aromatic amines
Lan Luo1, Yuguang Liu1, Wangsong Chen1
1State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing 100029, China.
Abstract:
Photoelectrocatalytic (PEC) strategy has emerged as a promising approach to drive organic reactions under mild conditions. Here, we present a protocol for PEC oxidative coupling of aromatic amines to produce aromatic azo compounds over a porous BiVO4 nanoarray (BiVO4-NA) photoanode. We describe the fabrication of BiVO4-NA photoanode and the detailed steps for the PEC oxidative coupling reaction, including key performance data of the BiVO4-NA photoanode for synthesizing azobenzene from aniline. For complete details on the use and execution of this protocol, please refer to Luo et al. (2022).1.
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