A Low-Cost Approach for Batch Separation, Identification and Quantification of Microplastics in Agriculture Soil

An increasing trend of research on microplastics (MPs) pollution in soil requires plenty of accurate data on MPs occurrence in soil samples. Efficient and economical methods of obtaining MP data are in development, especially for film MPs. We focused on MPs originating from agricultural mulching films (AMF) and presented an approach that can separate MPs in batches and identify them quickly. It mainly includes separation by ultrasonic cleaning and centrifugation, digestion of organic matter, and an AMF-MPs identification model. Adding olive oil or n-hexane to saturated sodium chloride constituted the best combination of separation solutions. Controlled experiments proved that the optimized methods improved the efficiency of this approach. The AMF-MPs identification model provides specific characteristics of MPs and can identify MPs efficiently. Evaluation results showed that the mean MP recovery rate reached 95%. The practical application demonstrated that this approach could conduct MPs analysis in soil samples in batches with less time and low cost.