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Updated: Jul 15, 2026

Protocol for Microplastics Sampling on the Sea Surface and Sample Analysis
Published on: December 16, 2016
A standard analytical approach and establishing criteria for microplastic concentrations in wastewater, drinking
Daniel Sol1, Carmen Solís-Balbín1, Amanda Laca1
1Department of Chemical and Environmental Engineering, University of Oviedo, C/ Julián Clavería s/n, 33006 Oviedo, Spain.
Abstract:
The ubiquitous presence of microplastics (MPs) in natural water bodies reflects the global issue regarding these micropollutants. The main problem of MPs lies on the difficulty of removing these particles from water during wastewater and drinking water treatments. The release of MPs to the environment in treated wastewater contributed to the dispersion of these micropollutants, which enhances the harmful effect of MPs on fauna and flora. In addition, their presence in tap water entails a potential risk to human health since MPs can be directly consumed. The first step is being able to quantify and characterise these microparticles accurately. In this work, a comprehensive analysis on the presence of MPs in wastewater, drinking water and tap water has been conducted with emphasis on sampling methods, pre-treatment, MP size and analytical methods. Based on literature data, a standard experimental procedure has been proposed with the objective of recommending a methodology that allows the homogenisation of MP analysis in water samples. Finally, reported MP concentrations for influents and effluents of drinking and wastewater treatment plants and tap water have been analysed, in terms of abundance, ranges and average values, and a tentative classification of different waters based on their MP concentrations is proposed.
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