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Preparation and Reactions of Sulfides02:26

Preparation and Reactions of Sulfides

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Sulfides are the sulfur analog of ethers, just as thiols are the sulfur analog of alcohol. Like ethers, sulfides also consist of two hydrocarbon groups bonded to the central sulfur atom. Depending upon the type of groups present, sulfides can be symmetrical or asymmetrical. Symmetrical sulfides can be prepared via an SN2 reaction between 2 equivalents of an alkyl halide and one equivalent of sodium sulfide.
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Liquid-Phase Approach to Glass-Microfiber-Reinforced Sulfide Solid Electrolytes for All-Solid-State Batteries.

Hany El-Shinawi1,2,3, Ed Darnbrough4,3, Johann Perera4,3

  • 1Department of Materials Science and Engineering, University of Sheffield, Mappin Street, Sheffield City Centre, Sheffield S1 3JD, United Kingdom.

ACS Applied Materials & Interfaces
|July 19, 2023
PubMed
Summary

Scalable sulfide solid-state batteries are enabled by new deformable glass-microfiber composites. This approach enhances energy density and simplifies thin membrane production for advanced battery applications.

Keywords:
glass microfibersolid electrolytessolid-state batteriessulfide electrolytesthin composites

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Area of Science:

  • Materials Science
  • Electrochemistry
  • Energy Storage

Background:

  • Deformable, fast-ion conducting sulfides are key for bulk-type solid-state batteries.
  • Optimizing energy density requires minimizing electrolyte layer thickness via thin membranes.
  • Current methods for thin, additive-free sulfide membranes face scalability and integration challenges.

Purpose of the Study:

  • To develop a scalable, solution-based method for producing reinforced sulfide solid electrolyte composites.
  • To restore deformability to sulfide electrolytes for easier processing.
  • To enhance the energy density and manufacturability of sulfide-based solid-state batteries.

Main Methods:

  • A solution-based approach was used to create glass-microfiber-reinforced sulfide composites.
  • The composites were shaped into thin membranes using cold pressing.
  • The deformability and processability of the new composite material were evaluated.

Main Results:

  • The proposed method yields bulk-type, deformable sulfide electrolyte composites.
  • Thin membranes can be readily produced via cold pressing.
  • The approach facilitates large-scale production and integration into solid cells.

Conclusions:

  • Scalable production of deformable sulfide electrolytes is achievable through glass-microfiber reinforcement.
  • This method simplifies the fabrication of thin membranes, boosting energy density.
  • The composite approach offers a promising route for practical sulfide-based solid-state batteries.