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A precision dimple grinder-polisher produced by 3D printing.

Lawrence Whitmore1

  • 1Department of Chemistry and Physics of Materials, Paris Lodron University of Salzburg (PLUS), Jakob-Haringer Strasse 2a, Salzburg 5020, Austria.

Ultramicroscopy
|August 4, 2023
PubMed
Summary

A novel 3D-printed grinder-polisher creates thin sample areas for transmission electron microscopy. This cost-effective, sustainable device aids scientific research and teaching labs.

Keywords:
3d printingDimple grindingSample preparationSustainable developmentTransmission electron microscopy

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Area of Science:

  • Materials Science
  • Engineering
  • Microscopy

Background:

  • Preparing samples for transmission electron microscopy (TEM) often requires specialized equipment.
  • Achieving thin central areas in 3 mm round samples is crucial for subsequent ion milling to electron transparency.
  • Laboratories need accessible and cost-effective solutions for sample preparation.

Purpose of the Study:

  • To design and construct a precision grinder-polisher using 3D printing technology.
  • To enable laboratories to self-fabricate a device for preparing TEM samples.
  • To promote sustainable development goals in labs through recycling and biodegradable materials.

Main Methods:

  • A 3D-printed precision dimple grinder-polisher was designed and constructed.
  • Novel sample holder for alignment without a monocular and thickness detection via light transmission was developed.
  • Solutions for aligning motors and fixing polishing cloths were implemented.
  • Investigation of diameter-depth relationships for steel and plastic grinding discs was performed.
  • Samples of copper, silicon, and tungsten were prepared and examined using TEM.

Main Results:

  • The 3D-printed grinder-polisher successfully produces thin central areas in 3 mm round samples.
  • The novel sample holder design simplifies alignment and thickness detection.
  • The device is adaptable for various materials, including copper, silicon, and tungsten.
  • Evaluation in TEM confirmed the quality of the prepared samples.

Conclusions:

  • A cost-effective, self-buildable 3D-printed grinder-polisher is presented for TEM sample preparation.
  • The device offers a sustainable solution for research and teaching laboratories.
  • The design incorporates novel features for improved sample handling and alignment.