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Data reduction for spatially resolved reflectance anisotropy spectrometer.

L Rodríguez-Salas, A Lastras-Martínez, O F Núñez-Olvera

    The Review of Scientific Instruments
    |October 2, 2023
    PubMed
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    Ratio-based multi-level resistive memory cells.

    Scientific reports·2021
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    Off-axis rays in reflectance anisotropy (RA) spectrometers create false signals. A new data-reduction method using singular value decomposition effectively removes these spurious RA signals.

    Area of Science:

    • Spectroscopy
    • Optical Physics
    • Materials Science

    Background:

    • Spatially resolved reflectance anisotropy (RA) spectroscopy is a powerful technique for analyzing material properties.
    • Off-axis optical rays in RA spectrometers can introduce uncorrected signal artifacts.
    • These artifacts arise from the difference in s- and p-polarized reflectivity and depend on the light's incidence position.

    Purpose of the Study:

    • To identify and remove spurious signals caused by off-axis rays in spatially resolved RA measurements.
    • To develop a robust data-reduction procedure for accurate RA spectroscopy.
    • To validate the proposed method with a novel spectrometer design.

    Main Methods:

    • Singular value decomposition (SVD) analysis of spatially resolved RA spectra.

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  • Development of a spatially resolved RA spectrometer utilizing an 8x8 multi-anode photomultiplier (PMT).
  • Implementation of phase-sensitive detection techniques to improve signal-to-noise ratio.
  • Main Results:

    • A data-reduction procedure was developed to effectively identify and remove spurious RA signals originating from off-axis rays.
    • The proposed method successfully corrects for artifacts independent of optical alignment.
    • The use of an 8x8 multi-anode PMT enabled enhanced signal-to-noise ratios crucial for evaluating the data reduction procedure.

    Conclusions:

    • Off-axis rays in RA spectrometers introduce a complex, uncorrectable artifact.
    • Singular value decomposition provides an effective method for removing these spurious signals.
    • The developed data-reduction procedure and spectrometer design enhance the accuracy and reliability of spatially resolved RA measurements.