One-Dimensional Nickel Molybdate Nanostructures with Enhanced Supercapacitor Performance

One-dimensional NiMoO₄ nanofibers were successfully prepared by electrospinning and high-temperature calcination. The supercapacitor performance tests were conducted on the prepared materials in a three-electrode system, and it was found that the calcination temperature during the preparation of the fibers seriously affects the final morphology and electrochemical performance of the obtained samples. The sample with a calcination temperature of 500 °C has better performance, its specific capacitance can reach 1947 F g^-1, and the retention rate is 82.35% after 3000 cycles of constant current charging-discharging. The improvement of electrochemical performance is primarily on account of the unique one-dimensional nanostructure of the material, which can both enhance the charge transfer efficiency and effectively increase the speed of electrolyte ion diffusion.